Equipment

Two high-resolution pulse NMR spectrometers are avialable in our laboratory:

Bruker 600 Avance^III

Triple-resonance digital NMR spectrometer with the following parameters:

• actively shielded superconducting magnet UltraShield™ 14.1 T
• digital console
• orthogonal BOSS II shimming system with 34 gradients
• two probeheads:
  • 5 mm triple-resonance cryoprobe TCI (¹H observe, ¹³C and ¹⁵N manipulation, deuterium decoupling possible), actively shielded z-gradient
  • 5 mm TXI – triple-resonance probehead for inverse experiments (¹H observe, ¹³C and ¹⁵N manipulation), actively shielded z-gradient

Bruker Avance III 500 MHz

in the configuration as a two-channel high performance Fourier NMR spectrometer equipped with

• gradient unit in z-axis
• fully digital console Avance III
• Bruker shim system BOSS 3
• three special probeheads
  • 5 mm BBFO probehead for direct observation of ¹H, ¹⁵N-³¹P (39-162 MHz) and ¹⁹F nuclei with decoupling of ¹H or ¹⁹F nuclei
  • inverse 5 mm BBI probehead (¹H observe, BB/¹³C decoupling) with z-gradient
  • 10 mm broadband probehead in the standard range (³¹P - ¹⁰⁹Ag), ¹H decoupling