Protokoly z XRD difraktometrů
Semikvantitativní analýza korozních produktů Fe pomocí „korundových čísel“, neuvažuje amorfní podíl. Pro vzorky s Fe a Co je vhodná Co-lampa.
|
Ref. Code |
Score |
Comp.Name |
Mineral Name |
Chem. Formula |
SemiQuant [%] |
|
04-015-8209 |
59 |
Iron Oxide |
Magnetite |
Fe3 O4 |
Cca 25 |
|
04-015-8205 |
61 |
Iron Oxide Hydroxide |
Goethite |
Fe O ( O H ) |
Cca 40 |
|
01-074-6247 |
52 |
Iron Oxide Hydroxide |
Lepidocrocite, syn |
Fe O ( O H ) |
Cca 25 |
|
04-015-9760 |
35 |
Iron Carbonate |
Siderite, syn |
Fe ( C O3 ) |
Cca 10 |
Kvantitativní Rietveldova analýza -stanovení amorfního podílu metodou vnitřního standardu ZnO=7.5%.
|
Ref.Code |
Score |
Comp. Name |
Mineral Name |
Chem. Formula |
Quant[%] |
|
01-079-1276 |
53 |
Aluminum Silicon Oxide |
Mullite, syn |
Al2(Al2.8 Si1.2)O9.6 |
30.8(2) |
|
01-070-8072 |
47 |
Zinc Oxide |
|
Zn O |
7.5 |
|
01-075-8320 |
42 |
Silicon Oxide |
Quartz |
Si O2 |
7.9(2) |
|
01-084-2782 |
36 |
Iron Oxide |
Magnetite |
Fe3 O4 |
2.06(2) |
|
01-071-1166 |
14 |
TitaniumOxide |
Anatase |
Ti O2 |
1.26(2) |
|
01-073-1765 |
25 |
TitaniumOxide |
Rutile, syn |
Ti O2 |
0.88(2) |
|
01-079-0007 |
36 |
Iron Oxide |
Hematite, syn |
Fe2 O3 |
1.26(2) |
|
|
|
Amorphous |
|
|
48.8(2) |
Stanovení velikost krystalitů Anatasu v různých krystalografických směrech metodou Wiliamson-Hall plot.
|
Pos. [°2Th.] |
d-spacing[A] |
Height [cts] |
R.I. [%] |
h k l |
Crys.Size[A] |
Matched by |
|
25.28(3) |
3.51939 |
33621(89) |
100.00 |
1 0 1 |
264 |
04-007-0701 |
|
|
|
|
|
|
|
|
|
36.90(1) |
2.43228 |
2126(36) |
6.32 |
1 0 3 |
248 |
04-007-0701 |
|
|
|
|
|
|
|
|
|
37.78(6) |
2.37944 |
8401(72) |
24.99 |
0 0 4 |
221 |
04-007-0701 |
|
|
|
|
|
|
|
|
|
38.60(3) |
2.33334 |
2618(325) |
7.79 |
1 1 2 |
252 |
04-007-0701 |
|
|
|
|
|
|
|
|
|
48.01(9) |
1.89322 |
15900(283) |
47.29 |
2 0 0 |
277 |
04-007-0701 |
|
|
|
|
|
|
|
|
|
53.9(3) |
1.70057 |
9319(84) |
27.72 |
1 0 5 |
227 |
04-007-0701 |
|
|
|
|
|
|
|
|
|
55.04(5) |
1.66717 |
10009(242) |
29.77 |
2 1 1 |
250 |
04-007-0701 |
|
|
|
|
|
|
|
|
|
62.00(5) |
1.49342 |
1458(370) |
4.34 |
2 1 3 |
292 |
04-007-0701 |
|
|
|
|
|
|
|
|
|
62.70(4) |
1.48124 |
7093(317) |
21.10 |
2 0 4 |
280 |
04-007-0701 |
|
|
|
|
|
|
|
|
|
69.00(1) |
1.36420 |
3235(296) |
9.62 |
1 1 6 |
202 |
04-007-0701 |
|
|
|
|
|
|
|
|
|
70.00(1) |
1.33872 |
3511(47) |
10.44 |
2 2 0 |
216 |
04-007-0701 |
|
|
|
|
|
|
|
|