Two high-resolution pulse NMR spectrometers are avialable in our laboratory:
Bruker 600 AvanceIII
Triple-resonance digital NMR spectrometer with the following parameters:
- actively shielded superconducting magnet UltraShield™ 14.1 T
- digital console
- orthogonal BOSS II shimming system with 34 gradients
- two probeheads:
- 5 mm triple-resonance cryoprobe TCI (1H observe, 13C and 15N manipulation, deuterium decoupling possible), actively shielded z-gradient
- 5 mm TXI – triple-resonance probehead for inverse experiments (1H observe, 13C and 15N manipulation), actively shielded z-gradient
Bruker Avance III 500 MHz
in the configuration as a two-channel high performance Fourier NMR spectrometer equipped with
- gradient unit in z-axis
- fully digital console Avance III
- Bruker shim system BOSS 3
- three special probeheads
- 5 mm BBFO probehead for direct observation of 1H, 15N-31P (39-162 MHz) and 19F nuclei with decoupling of 1H or 19F nuclei
- inverse 5 mm BBI probehead (1H observe, BB/13C decoupling) with z-gradient
- 10 mm broadband probehead in the standard range (31P - 109Ag), 1H decoupling
